Synthesis of Substituted Resorcinol Monomethyl Ethers from 2-Bromo-3-methoxycyclohex-2-en-1-ones
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Shao, W., & Clive, D. L. J. (2016). Synthesis of substituted resorcinol monomethyl ethers from 2-bromo-3-methoxycyclohex-2-en-1-ones. Journal of Organic Chemistry, 80(6), 3211–3216. https://doi-org.login.ezproxy.library.ualberta.ca/10.1021/acs.joc.5b00192
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2-Bromo-3-methoxycyclohex-2-en-1-ones are readily alkylated at C-6 with
reactive halides, and then treatment with DBU (2 equiv) in PhMe at room temperature results in
smooth loss of bromide and aromatization to resorcinol (monomethyl ethers of defined
substitution pattern.
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http://purl.org/coar/resource_type/c_6501 http://purl.org/coar/version/c_b1a7d7d4d402bcce http://purl.org/coar/version/c_71e4c1898caa6e32
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This document is the Accepted Manuscript version of a Published Work that appeared in final form in Journal of Organic Chemistry, copyright © 2015 American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see https://doi.org/10.1021/acs.joc.5b02187.
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en